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October 06, 2009

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February 11, 2009

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LCPP-CNRS/ESCPE

Bât. F308, B.P. 2077
43 Bd du 11 Nov. 1918
69616 Villeurbanne cedex
FRANCE

  Laboratoire de Chimie et Procédés de Polymérisation


Equipment



Polymerisation Reactors and Equipment

Numerous high pressure cylindrical reactors (60b) for slurry phase olefin polymerisation ( 1 )
2.5 litre reaction calorimetery with temperature control (up to 22 bars) ( 2 )
2.5 litre “Turbosphere” Reactor for gas phase olefin polymerisation (up to 22 bars) ( 3 )
Numerous 0.5l glass reactors for low pressure polymerization ( 4 )
Gas phase and slurry phase stopped flow reactors for olefin polymerisation.
Rapid (40 millisecond) polymerisation under industrial conditions.
 ( 5 - 6 )
High purity glove box for catalyst preparation ( 7 )
High pressure emulsion polymerisation 
Flexible tubular reactors for latex preparation (up to 80m) ( 8 )
High vacuum system / oven for solid catalyst preparation 
Numerous argon/vacuum lines for organometallic synthesis 









Characteristion and Analysis

High Temperature GPC in TCB (150°C) for polyolefins. ( 9 )
Solution (THF) and aqueous GPC.
Differential Scanning Calorimetry (2)
Infrared Spectroscope (MIR).
RFS Rheometry (for latex products) ( 10 )
Access to NMR liquid (400 MHz) and solid (500 MHz), MALDI-ToF MS
UV Spectroscope
Quasi-elastic light scattering: ZetaSizer 1000 (90°) and AutoSizer 4800 (Variable Angle)
Static light scattering (full PSD): LS 230 (Coulter) ( 11 )
Sieves for dry powders with dp> 1 µm.





Other Characterisation Techniques Available

High Speed Centrifuge.
Tensiometry
Conducitivity
Gas Phase Chromatography ( 12 )






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